Oral 23rd International Society of Magnetic Resonance Conference 2023

Structure-based design of constrained peptides targeting undruggable targets in cardiovascular disease and cancer (#151)

Conan K Wang 1
  1. The University of Queensland, St Lucia, QLD, Australia

Background: Many proteins are considered ‘undruggable’ because of their large, flat, and featureless target interfaces. Constrained peptides, which fill a gap between classical small molecules and large antibody therapeutics, have potential to inhibit these challenging protein targets with high specificity. However, effective design strategies to capture the therapeutic potential of peptides are still needed to enable development of new drugs leads and for their translation.

 

Aims and Methods: We employ approaches guided by structure. (i) The first approach involved analysis of target surface structure to identify cryptic sites and further optimisation to improve stability [1, 2]. (ii) The second approach was based on structure mimicry of an endogenous binding partner and grafting onto an ultrastable disulfide-rich peptide scaffold [3]. We investigated two difficult-to-inhibit targets, PCSK9 for lowering cholesterol and preventative cardiovascular care, and PD-L1 for modulation of immune checkpoint inhibitors and cancer treatment.

 

Results: To validate our structure-based approaches we heavily rely on solution NMR. Activity was validated using a series of in vitro (SPR, ITC, ELISA), cellular, and in vivo assays. We successfully generated potent lead peptides with affinities in the pico- to nanomolar range [1, 2, 3]. 

 

Significance: The success of the strategies in generating potent peptide inhibitors suggest they could be of broad interest, as many protein-protein interactions remain underexplored due to their challenging topological nature. Indeed, a bioinformatic analysis of the peptide:protein structures indicated our cyclisation approach could have broad utility. At present, there are >60 peptide drugs in market with peptide drugs being activity pursued by all major pharmaceutical companies. 

  1. Tombling BJ, Lammi C, Lawrence N, Gilding EK, Grazioso G, Craik DJ, Wang CK. Bioactive Cyclization Optimizes the Affinity of a Proprotein Convertase Subtilisin/Kexin Type 9 (PCSK9) Peptide Inhibitor. J Med Chem 2020. 64:2523-33.
  2. Zhang Y, Wang L, Tombling BJ, Lammi C, Huang YH, Li Y, Bartolomei M, Hong, B, Craik DJ, Wang CK. Improving Stability Enhances In Vivo Efficacy of a PCSK9 Inhibitory Peptide. J Am Chem Soc 2022. 144: 19485-19498.
  3. Yin H, Zhou X, Huang YH, King GJ, Collins BM, Gao Y, Craik DJ, Wang CK. Rational Design of Potent Peptide Inhibitors of the PD-1:PD-L1 Interactions for Cancer Immunotherapy. J Am Chem Soc 2020 143:18536-18547.